Propylene glycol methyl ether → Propylene glycol methyl ether

HRID 1421455Notes

Reaction equation

HRID 1421455 reaction equation
[Al].[CH3:2][O:3][CH:4]([OH:7])[CH2:5][CH3:6]>CN(C=O)C>[OH:7][CH2:4][C:5]1[C:6]([CH3:4])=[CH:6][CH:5]=[C:6]([OH:7])[C:5]=1[CH2:4][OH:7].[CH3:2][O:3][CH:4]([OH:7])[CH2:5][CH3:6]

Participants

5

Reactant 2

HCID 3032390Propylene glycol methyl ether2×HCID 5359268Aluminum

Product 2

HCID 3032390Propylene glycol methyl etherHCID 21641889HCID 21641889, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent2×

Procedure

A solution containing 1.18 g of 40% w/w novolak B in methoxypropanol, 0.14 g of a 40% solution of bis(hydroxymethyl)p-cresol in methoxypropanol, 0.055 g of a 10% solution of acid generator C in DMF, 0.022 g of dye A, 1.42 g of methoxypropanol and 1.96 g of DMF was prepared and coated onto a substrate consisting of a sheet of aluminium that had been electrograined and anodised, giving a coating film weight of 1.3 gm-2 after thoroughly drying at 100° C. in an oven for 3 minutes.

Workup

  1. customgiving a coating film weight of 1.3 gm-2
  2. customafter thoroughly drying at 100° C. in an oven for 3 minutes

Sources & evidence

ORD record
ord-d8fecc0b775442419fd757032b763d83
Source dataset
uspto-grants-2000_06
Patent number
US06077641

Reaction notes

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