HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 4-(4-Chlorobenzoyl)benzyl bromide | HCID 9839651 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide | HCID 18779877 | 85.4% |
Reaction Steps
An acetone solution (500 ml) of 4-bromomethyl-4'-chlorobenzophenone (31 g) and thiourea (10 g) was heated for 30 minutes with refluxing. The precipitated crystals were then collected by filtration and washed with acetone to obtain S-(4-(4-chlorobenzoyl)benzyl)thiouronium bromide (33 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06077866 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-856fc1cebc144e7eb88891a8c8c5cbd4 |
| Source note | uspto-grants-2000_06 |