Hydrochloric Acid → HCID 86755469, compound

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Reaction Steps

A mixture of N-neohexyl-L-aspartic acid dimethyl ester (15 g, 0.061 mol) in 1N hydrochloric acid (350 mL) was heated at reflux for 4 hours to form a clear solution. The mixture was freeze dried to give N-neohexyl-L-aspartic acid hydrochloride as a white solid (14 g, 91%), M.P. 133-138° C., [α]D +14.69 (c=1, water). Anal. Calc'd. for C10H19NO4 --HCl; C, 47.52; H, 7.92; N, 5.54; Cl, 14.05. Found: C, 47.84; H, 8.14; N, 5.31; Cl, 13.08.

Provenance & Evidence