HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → HCID 18706217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | Hexamethyldisiloxane | HCID 24764 | — |
| Reactant | 1-Propanol, 2-(decyloxy)-3-(dodecylthio)- | HCID 11825883 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18706217 | HCID 18706217 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
A suspension of 4.26 g P4O10 in 60 ml absolute pyridine was admixed at room temperature with 13 ml hexamethyldisiloxane and heated to 100° C. for 1 hour. It was then slightly cooled, admixed with 25 g 3-dodecylmercapto-2-decyloxy-1-propanol and heated for a further 2.5 hours to 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06080734 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-7feecf3472544bf299f262297310d1a6 |
| Source note | uspto-grants-2000_06 |