HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131721862, compound → HCID 86755472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131721862 | HCID 131721862 | — |
| Reactant | HCID 178418435 | HCID 178418435 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86755472 | HCID 86755472 | — |
Reaction Steps
Estrone-(N-methyl)amidosulphonate (1 g) is reduced with sodium boron hydride (624.2 mg) in a mixture of tetrahydrofurane (20 ml) and methanol (20 ml). The crude product, following work-up, is recrystallised from acetone/n-hexane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06080735 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-546fd987d56748a0a134d63717a02bf3 |
| Source note | uspto-grants-2000_06 |