HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichlorobenzene → HCID 18707312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichlorobenzene | HCID 7239 | — |
| Reactant | HCID 18707198 | HCID 18707198 | — |
| Product | HCID 18707312 | HCID 18707312 | — |
Reaction Steps
A solution of 1 g of 2-(3,4-diethoxyphenyl)-4-(4-allyloxy-3-methoxycarbonylphenyl)thiazole in 25 ml of o-dichlorobenzene was refluxed for 15 hours with heating. After the completion of a reaction, the solvent was removed by distillation. The residue was recrystallized from diisopropyl ether to obtain 1 g of 2-(3,4-diethoxyphenyl)-4-(3-methoxycarbonyl-4-hydroxy-5-allylphenyl)thiazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06080764 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-403e62e48f774194a77d5b0122c73c94 |
| Source note | uspto-grants-2000_06 |