HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54045910, compound → HCID 53974404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54045910 | HCID 54045910 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53974404 | HCID 53974404 | 113% |
Reaction Steps
4-Ethyl-3-(4-benzyloxyphenyl)pyrrolo[2,1,5-cd]indolizine-2-carboxylic acid dimethlamide was hydrogenated by the general synthetic principles outlined in example 12, to afford 4-ethyl-3-(4-hydroxyphenyl)pyrrolo[2,1,5-cd]indolizine-2-carboxylic acid dimethylamide as a yellow gum in 113% yield (ethanol incl.). 1H-NMR (CDCl3, 300 MHz) δ: 1.43 (t, 3H); 2.56 (s, 3H); 2.98 (s, 3H); 3.19 (q, 2H); 7.00 (d, 2H); 7.33 (s, 1H); 7.49 (d, 2H); 7.68 (dd, 1H); 7.96 (d, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06080754 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-6766a20ac61e41a292f5fd0c97383b9e |
| Source note | uspto-grants-2000_06 |