Trityl chloride → HCID 18779112, compound

Participants

Reaction Steps

To a cold (0° C.) solution of 4-(4-cyanophenyloxy)-imidazole (155 mg, 0.84 mmol) and triethylanine (0.129 mL, 0.92 mmol) in DMF (1 mL) was added trityl chloride (245 mg, 0.88 mmol). The resultant mixture was stirred at ambient temperature for 5 days. The product mixture was concentrated onto silica gel, chromatographed (Silica gel, 1:9 acetone in CHCl3) to afford the title compound as a white powder.

Provenance & Evidence