Pyridine → 1-Butylpyridinium bromide

HRID 1422463Notes

Reaction equation

HRID 1422463 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH3:5].[N:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[Br-:1].[CH2:2]([N+:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 1049PyridineHCID 8002Butyl bromide

Product 1

HCID 27342381-Butylpyridinium bromide

Procedure

Butylpyridinium bromide is prepared by a Menshutkin reaction of 27.5 g of 1-bromobutane with 15.8 g of pyridine at 40° C. in 24 hours, without solvent. The solid obtained is dried under low vacuum at 50° C.

Workup

  1. customThe solid obtained
  2. customis dried under low vacuum at 50° C.

Sources & evidence

ORD record
ord-f6f3807a53504064978aa6558408ba26
Source dataset
uspto-grants-2015_01
Patent number
US08927160B2

Reaction notes

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