HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → HCID 72208044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 2,4-Dichloro-7H-pyrrolo[2,3-d]pyrimidine | HCID 14116871 | — |
| Product | HCID 72208044 | HCID 72208044 | — |
Reaction Steps
Following the procedure of Example 15b, 2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine (0.5 g, 2.67 mmol) was reacted with 2-iodopropane. The crude residue was purified by silica gel chromatography (15 to 25% ethyl acetate in hexane eluant) to afford the title compound as a solid. MS m/z 230.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927281B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-2c44590765da43feb1e2242d60338787 |
| Source note | uspto-grants-2015_01 |