HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 53468631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | HCID 53468223 | HCID 53468223 | — |
| Catalyst | Mercuric Chloride | HCID 24085 | — |
| Solvent | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Product | HCID 53468631 | HCID 53468631 | 58% |
Reaction Steps
This compound was prepared according to the method described for the compound 6a employing 9d (764.89 mg, 1.0 mmol) and HgCl2 (582 mg, 2.26 mmol), CaCO3 (230 mg, 2.46 mmol) in acetonitrile-water (4:1) to obtain the pure product 10d (373 mg, 58% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927538B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-088604227a034f529999bd8e20fbb6ee |
| Source note | uspto-grants-2015_01 |