HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68345601, compound → HCID 68345602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68345601 | HCID 68345601 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68345602 | HCID 68345602 | — |
Reaction Steps
The title product is prepared from 1-(4-fluorophenyl)-1H-pyrazolo[3,4-d]pyridazine-4-carboxylic acid ethyl ester (520 mg, 1.82 mmol) according to the procedure described in Example 1, with the exception that the reaction progress is monitored for the disappearance of the starting material by TLC (EtOAc:hexanes; 1:1) prior to work up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927550B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-f522d23b5eb44531a7c2b8a473a06144 |
| Source note | uspto-grants-2015_01 |