Hydrochloric Acid → HCID 87126777, compound

Participants

Reaction Steps

To a mixture of 2-methyl-propane-2-sulfinic acid [(S)-1-(6-bromopyridin-3-yl)-propyl]-amide (5.35 g, 16.8 mmol) in methanol (25 mL) is added a solution of 4 N HCl in dioxane (10 mL, 40 mmol). After 2 hour, the mixture is concentrated to near dryness to afford a white solid. The solid is diluted with ether and collected by filtration to afford the title compound.

Provenance & Evidence