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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1423087Generated: November 2, 2026

5-Bromo-2-methoxyphenol → HCID 66824716, compound

https://huagongshe.com/reaction/1423087

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Bromo-2-methoxyphenolHCID 142228—
Reactant1-Methyl-3-pyrrolidinol, (+)-HCID 643504—
ProductHCID 66824716HCID 6682471658.4%

Reaction Steps

The title compound was prepared by the method outlined for Preparative Example 63 using 5-bromo-2-methoxy-phenol (1.00 g, 4.926 mmol) and (S)-1-methyl-pyrrolidin-3-ol (601 mg, 5.94 mmol) to afford titled compound as a colorless solid (823 mg, 58%). LC/MS (Method B) 1.18 min, [M+1]+ 286/288.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08927546B2
Source datasetuspto-grants-2015_01
ORD IDord-b6a201e22a9a4ee88ecc570dc49d4347
Source noteuspto-grants-2015_01