HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-methoxyphenol → HCID 66824716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-methoxyphenol | HCID 142228 | — |
| Reactant | 1-Methyl-3-pyrrolidinol, (+)- | HCID 643504 | — |
| Product | HCID 66824716 | HCID 66824716 | 58.4% |
Reaction Steps
The title compound was prepared by the method outlined for Preparative Example 63 using 5-bromo-2-methoxy-phenol (1.00 g, 4.926 mmol) and (S)-1-methyl-pyrrolidin-3-ol (601 mg, 5.94 mmol) to afford titled compound as a colorless solid (823 mg, 58%). LC/MS (Method B) 1.18 min, [M+1]+ 286/288.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927546B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-b6a201e22a9a4ee88ecc570dc49d4347 |
| Source note | uspto-grants-2015_01 |