HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-methyl-1H-1,2,4-triazol-5-yl)acetic acid → HCID 178491987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-methyl-1H-1,2,4-triazol-5-yl)acetic acid | HCID 7019477 | — |
| Reactant | (S)-3-benzyl-1-[4-methoxy-3-(1-methyl-piperidin-4-yloxy)-phenyl]-piperazine dihydrochloride | HCID 66825019 | — |
| Product | HCID 178491987 | HCID 178491987 | 17% |
Reaction Steps
Prepared using the same procedure described in Example 189 from (S)-3-benzyl-1-[4-methoxy-3-(1-methyl-piperidin-4-yloxy)-phenyl]-piperazine dihydrochloride and (5-methyl-1H-[1,2,4]triazol-3-yl)-acetic acid to afford the title compound as colorless solid (20 mg, 17%). LC/MS (Method B) 2.10 min, [M+1]+ 519.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927546B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-82e037da24514ddf81391a16f959f342 |
| Source note | uspto-grants-2015_01 |