Iodoethane → 2-Bromo-1-ethoxy-4-(trifluoromethyl)benzene

HRID 1423398Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:5]=[CH:4][C:3]=1[OH:12].[CH2:13](I)[CH3:14]>>[Br:1][C:2]1[CH:7]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:5]=[CH:4][C:3]=1[O:12][CH2:13][CH3:14]

Participants

Reactant 2

HCID 6340Iodoethane

HCID 27611682-Bromo-4-(trifluoromethyl)phenol

Product 1

HCID 451586702-Bromo-1-ethoxy-4-(trifluoromethyl)benzene

Procedure

Starting from commercially available 2-bromo-4-trifluoromethyl-phenol and ethyliodide the title compound is obtained as colorless oil after distillation at 5×10−3 mbar.

Sources & evidence

ORD record: ord-da442cc4eaa549e1905b6a0d4463dda3
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08927557B2

Reaction notes

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