Bromomethylcyclopropane → HCID 67033133, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[C:6]([CH:8]([CH3:10])[CH3:9])[CH:5]=[CH:4][C:3]=1[OH:11].Br[CH2:13][CH:14]1[CH2:16][CH2:15]1>>[Br:1][C:2]1[CH:7]=[C:6]([CH:8]([CH3:9])[CH3:10])[CH:5]=[CH:4][C:3]=1[O:11][CH2:13][CH:14]1[CH2:16][CH2:15]1Participants
3
Procedure
Starting from 2-bromo-4-isopropyl-phenol (example B.a6) and commercially available bromomethyl-cyclopropane the title compound is obtained as colorless solid after short path distillation at 2×10−3 mbar.
Sources & evidence
- ORD record
- ord-7b0bd8e7f59f4a67aff19e357f766f71
- Source dataset
- uspto-grants-2015_01
- Patent number
- US08927557B2
Reaction notes
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