HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenylboronic acid → HCID 178498913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenylboronic acid | HCID 285645 | — |
| Reactant | HCID 178498908 | HCID 178498908 | — |
| Product | HCID 178498913 | HCID 178498913 | — |
Reaction Steps
6-(4-Fluoro-phenyl)-4-hydroxy-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester was prepared from 6-bromo-4-hydroxy-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester under conditions analogous to Example 7(a) using 4-fluoro-phenylboronic acid. 1H NMR (200 MHz, CDCl3): δ (ppm)=8.515 (s, 1H), 7.765 (d, 1H), 7.586 (m, 2H), 7.427 (d, 1H), 7.381-7.120 (m, 2H), 4.026 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927591B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-8b2156c583a04690a9929c0f14b2d10c |
| Source note | uspto-grants-2015_01 |