HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-butylbenzene-1,2-diamine → HCID 178440689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-butylbenzene-1,2-diamine | HCID 432708 | — |
| Reactant | (4S)-1-tert-Butoxycarbonyl-4-fluoro-L-proline | HCID 2756017 | — |
| Product | HCID 178440689 | HCID 178440689 | — |
Reaction Steps
The title compound was prepared according to Method 4 using N-Boc-cis-4-fluoro-L-proline and 4-tert-butyl-1,2-diaminobenzene. The final residue was washed with ethyl acetate and diluted with water, basified with saturated lithium hydroxide solution (pH=8), extracted with ethyl acetate and dried over anhydrous Na2SO4 and concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927587B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-a8394b0e07a44f0b87b4557d1e35e1d2 |
| Source note | uspto-grants-2015_01 |