HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-butylbenzene-1,2-diamine → HCID 178454207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-butylbenzene-1,2-diamine | HCID 432708 | — |
| Reactant | HCID 10687368 | HCID 10687368 | — |
| Product | HCID 178454207 | HCID 178454207 | — |
Reaction Steps
The title compound was prepared according to Method 4 Steps 1 and 2 using 5-(benzyloxy)-N-(tert-butoxycarbonyl)-L-norvaline and 4-tert-butyl-1,2-diaminobenzene. The crude product was purified by silica gel column chromatography eluting with 30-40% EtOAc in petroleum ether (430 mg, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927587B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-b24118d173c2439fa7a485ce5edc273d |
| Source note | uspto-grants-2015_01 |