Ammonium Hydroxide → HCID 86699115, compound

Participants

Reaction Conditions

Reaction Steps

(2S,3R)-tert-butyl 2-(6-(tert-butyl)imidazo[1,2-a]pyridin-2-yl)-3-methyl-4-oxoazetidine-1-carboxylate (Preparation 38) was dissolved in THF (10 mL) and excess 28% aqueous ammonium hydroxide solution (ca 3 mL) added. The reaction was stirred in a sealed vial at 50° C. for 18 hours. The solvent was removed in vacuo to afford 311 mg of the title compound.

Provenance & Evidence