HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Cyano-3-fluorophenyl)boronic acid → HCID 86699133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Cyano-3-fluorophenyl)boronic acid | HCID 2783130 | — |
| Reactant | 4-Bromo-3-chloro-2-nitroaniline | HCID 26599156 | — |
| Product | HCID 86699133 | HCID 86699133 | — |
Reaction Steps
The title compound was prepared according to Preparation 92 using 3-fluoro-4-cyanophenylboronic acid and 4-bromo-3-chloro-2-nitroaniline. The residue was purified using silica gel column chromatography eluting with 10-50% EtOAc in heptanes to afford a yellow solid (2.45 g, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927587B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-b5ef646abe7e4faaa8c16e3e56b8f233 |
| Source note | uspto-grants-2015_01 |