HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57660946, compound → HCID 57660944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57660946 | HCID 57660946 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57660944 | HCID 57660944 | — |
Reaction Steps
1.3 g (2.16 mmol) of (3) and 130 mg Pd/C (10%) in 50 ml methanol were stirred under a hydrogen atmosphere for 3 h. The reaction mixture was filtered over a pad of Celite and the solvent was evaporated to give crude (4) as oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927534B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-0cb63dffae5446d885256256befcc0c4 |
| Source note | uspto-grants-2015_01 |