HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium hydroxide → 3,5-Dimethylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium hydroxide | HCID 62750 | — |
| Reactant | 1-Iodo-3,5-dimethylbenzene | HCID 140924 | — |
| Solvent | Dichloromethane heptane | HCID 21907733 | — |
| Product | 3,5-Dimethylphenol | HCID 7948 | 96% |
Reaction Steps
Following general operating mode A, 3,5-dimethyliodobenzene (145 μL, 1.0 mmol) was reacted with cesium hydroxide to give the expected product in the form of a white solid with a yield of 96% (eluent: dichloromethane/heptane 20:80).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927779B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-663a83ab21a846edb3862a9811e4fccf |
| Source note | uspto-grants-2015_01 |