HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium hydroxide → 2'-Hydroxyacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium hydroxide | HCID 62750 | — |
| Reactant | 2'-Bromoacetophenone | HCID 75060 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | 2'-Hydroxyacetophenone | HCID 8375 | 83% |
Reaction Steps
Following general operating mode A, 2′-bromoacetophenone (199 mg, 1.0 mmol) was reacted with cesium hydroxide to give the expected product in the form of an oil with a yield of 83% (eluent: ethyl acetate/heptane 20:80).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927779B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-d9cf9657d5c74bd2a309b6ae23149e41 |
| Source note | uspto-grants-2015_01 |