HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobiphenyl → 4-Hydroxybiphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobiphenyl | HCID 7101 | — |
| Reactant | Cesium hydroxide | HCID 62750 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | 4-Hydroxybiphenyl | HCID 7103 | 90% |
Reaction Steps
Following general operating mode B, 4-bromobiphenyl (232 mg, 1.0 mmol) was reacted with cesium hydroxide to give the expected product in the form of a brown solid with a yield of 90% (eluent: ethyl acetate/heptane 20:80).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927779B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-5f608057189d404caba85d86233e4dfe |
| Source note | uspto-grants-2015_01 |