HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoanisole → 3-Methoxyphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoanisole | HCID 16971 | — |
| Reactant | Cesium hydroxide | HCID 62750 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | 3-Methoxyphenol | HCID 9007 | 85% |
Reaction Steps
Following general operating mode B, 3-methoxybromobenzene (127 μL, 1.0 mmol) was reacted with cesium hydroxide to give the expected product in the form of an oil with a yield of 85% (eluent: ethyl acetate/heptane 10:90).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927779B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-c637ca45c58945a893f6b7571c382e82 |
| Source note | uspto-grants-2015_01 |