HRID1425616

反应详情

EQUATION

反应方程式

HRID 1425616 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Lithium 2,6-naphthalenedicarboxylate was synthesized by repeating the procedure of Experimental Example 1. The starting materials used were 2,6-naphthalenedicarboxylic acid and lithium hydroxide monohydrate (LiOH.H2O). Methanol (100 mL) was added to lithium hydroxide monohydrate (0.556 g), and it was stirred. After the lithium hydroxide monohydrate was dissolved, 2,6-naphthalenedicarboxylic acid (1.0 g) was added, and it was stirred for one hour. After stirring, the solvent was removed, and the residue was dried in vacuo at 150° C. for 16 hours to yield a white powder sample.

WORKUP

后处理

  1. stirringit was stirred for one hour
  2. stirringAfter stirring
  3. customthe solvent was removed
  4. customthe residue was dried in vacuo at 150° C. for 16 hours
  5. customto yield a white powder sample