Methyl 10-methylacridan-9-carboxylate → HCID 68467549, compound

HRID 1425640Notes

Reaction equation

HRID 1425640 reaction equation
CN1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]([C:16](Cl)=O)[C:8]2[CH:7]=[CH:6][CH:5]=CC1=2.[CH3:19][N:20]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:27]([C:34]([O:36]C)=[O:35])[C:26]2[CH:25]=[CH:24][CH:23]=[CH:22][C:21]1=2>ClCCl.O1CCCC1>[CH3:19][N:20]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:27]([C:34]([OH:36])=[O:35])[C:26]2[CH:25]=[CH:24][CH:23]=[CH:22][C:21]1=2.[CH:13]1[CH:12]=[CH:11][C:10]([C:9]2[CH:16]=[CH:5][CH:6]=[CH:7][CH:8]=2)=[CH:15][CH:14]=1

Participants

5

Reactant 2

HCID 12813956Methyl 10-methylacridan-9-carboxylateHCID 5452072910-Methylacridan-9-carboxylic acid chloride

Product 1

HCID 68467549HCID 68467549, compound

Reagents, catalysts & solvents 2

HCID 6344DichloromethaneSolvent2×HCID 8028TetrahydrofuranSolvent

Procedure

A solution of 0.24 parts of 10-methylacridan-9-carboxylic acid chloride (78) in 10 mL dichloromethane and 0.145 parts of 4-phenylphenol (76) in 5 mL of dichloromethane and 1 mL of tetrahydrofuran is treated as described in example I, to give 0.21 parts of 4,4′-biphenyl 10-methylacridan-9-carboxylate. This compound has the following structure.

Sources & evidence

ORD record
ord-5714e84936f8401590d7efef2601e888
Source dataset
uspto-grants-2015_01
Patent number
US08932881B2

Reaction notes

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