HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfone → HCID 67997575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfone | HCID 6213 | — |
| Reactant | 4-Bromo-2-fluoropyridine | HCID 2762851 | — |
| Product | HCID 67997575 | HCID 67997575 | 91% |
Reaction Steps
The title compound was prepared from 4-bromo-2-fluoro-pyridine and dimethylsulfone following a procedure analogous to that described in Step 1 for Intermediate 14. Yield: ca. 91% of theory (crude); LC (method 3): tR=2.01 min; Mass spectrum (ESI+): m/z=250/252 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933072B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-cd24551ba2ae47018b33835e2265f0ac |
| Source note | uspto-grants-2015_01 |