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HRID1426019

反应详情

EQUATION

反应方程式

HRID 1426019 的结构方程式

REACTANTS

反应物

2
结构：Brc1cnn(C2CCOCC2)c1
HCID51063926

4-Bromo-1-(oxan-4-yl)-1H-pyrazole

C8H11BrN2O

结构：C[C@@H](c1ccc(B2OC(C)(C)C(C)(C)O2)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2)OC1=O
HCID59532385

(S)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-3-((S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)-1,3-oxazinan-2-one

C28H38BNO5

PRODUCTS

生成物

1
结构：C[C@@H](c1ccc(-c2cnn(C3CCOCC3)c2)cc1)N1CC[C@](CC(C)(C)O)(c2ccccc2)OC1=O
HCID70651285

未命名化合物

收率 18%

PROCEDURE

实验过程

The title compound was prepared from (S)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-3-{(S)-1-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-ethyl}-1,3-oxazinan-2-one and 4-bromo-1-(tetrahydro-pyran-4-yl)-1H-pyrazole following a procedure analogous to that described in Example 1. Yield: 18% of theory; LC (method 3): tR=2.98 min; Mass spectrum (ESI+): m/z=504 [M+H]+.