HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)aniline → HCID 85984633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)aniline | HCID 66038 | — |
| Reactant | 4,6-Dichloropyrimidine-5-carbonitrile | HCID 599371 | — |
| Product | HCID 85984633 | HCID 85984633 | — |
Reaction Steps
Intermediate 4-chloro-6-(4-methylsulfanyl-phenylamino)-pyrimidine-5-carbonitrile was prepared in a similar manner as described herein using 4,6-dichloro-pyrimidine-5-carbonitrile and 4-methylsulfanyl-phenylamine. 1H-NMR (DMSO-d6): 10.22 (1H, s), 8.53 (1H, s) 7.43 (2H, m), 7.40 (2H, m), 2.49 (3H, s) ppm. LCMS: 277.0, 234.0, 149.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933083B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-479b761fbcc14a9c928e9511431f219e |
| Source note | uspto-grants-2015_01 |