HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluorobenzenesulfonyl chloride → HCID 67396338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluorobenzenesulfonyl chloride | HCID 2736911 | — |
| Reactant | HCID 67396538 | HCID 67396538 | — |
| Product | HCID 67396338 | HCID 67396338 | — |
Reaction Steps
By an operation similar to that in Reference Example 32 and using tert-butyl {[5-(2-fluoropyridin-3-yl)-1H-pyrrol-3-yl]methyl}methylcarbamate (305 mg), and 2,5-difluorobenzenesulfonyl chloride (319 mg), the title compound was obtained as a colorless oil (yield 160 mg, 33%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08933105B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-7838a570e8ef4836a7712f9081409c15 |
| Source note | uspto-grants-2015_01 |