Toluene → HCID 69082691, compound

Participants

Reaction Steps

0.43 g (2.31 mmoles) of 1-dodecyl alcohol are added to a toluene solution containing 0.22 g (0.76 mmoles) of 7-methyl-9-oxo-9H-thioxanthene-1-carbonyl chloride. After stirring 1 hour at room temperature, the mixture is poured in water, the organic phase is separated and washed with water. After evaporation of the solvent the oil is purified by flash chromatography (SiO2—eluent: Petroleum Ether:AcOEt 8:2) obtaining 50 mg of a yellow solid.

Provenance & Evidence