Hydrochloride methanol → 1-(3-(4-chlorophenyl)-1,1,1-trifluoropentan-3-yl)-1H-indazol-4-amine

Participants

Role	Name	HCID	Charge
Reactant	Hydrochloride methanol	HCID 21893726	—
Reactant	tert-butyl 1-(3-(4-chlorophenyl)-1,1,1-trifluoropentan-3-yl)-1H-indazol-4-ylcarbamate	HCID 70586827	—
Product	1-(3-(4-chlorophenyl)-1,1,1-trifluoropentan-3-yl)-1H-indazol-4-amine	HCID 70576682	—

Reaction Steps

A mixture of the product of Step E (80 mg, 0.17 mmol) and 4 N HCl/MeOH (2 mL) was stirred at room temperature for 2 h. After removing the solvent, the residue was dried in vacuo to give the title compound as colorless oil. LC/MS m/z=368.1[M+H]+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08933113B2
Source dataset	uspto-grants-2015_01
ORD ID	ord-82951150060f44158cae793835a61f4a
Source note	uspto-grants-2015_01