Nitromethane → HCID 72709581, compound

HRID 1427682Notes

Reaction equation

HRID 1427682 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8](=[O:11])[C:7]2=[O:12].[N+:13]([CH3:16])([O-:15])=[O:14]>O>[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8](=[O:11])[C:7]2([OH:12])[CH2:16][N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 6375NitromethaneHCID 3441357-Chloroisatin

Product 1

HCID 72709581HCID 72709581, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
30 °C

Procedure

7-chloroisatin (0.09 g) and nitromethane (0.1 ml) were added to water and the reaction mixture was vigorously stirred at a temperature of 30° C. for 24 hours. The obtained product was extracted with ethyl acetate and the solvent was removed to give pure product.

Workup

  1. extractionThe obtained product was extracted with ethyl acetate
  2. customthe solvent was removed
  3. customto give pure product

Sources & evidence

ORD record
ord-f9c93501a827425c888c9d5ebf8eb087
Source dataset
uspto-grants-2015_01
Patent number
US08933248B2

Reaction notes

Loading…