Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | 5-Nitroisatin | HCID 4669250 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 72709585 | HCID 72709585 | — |
Reaction Steps
5-nitroisatin (0.081 g) and nitromethane (0.15 ml) were added to water (2 ml) and the reaction mixture was vigorously stirred at a temperature of 30° C. for 12 hours. The product was extracted with ethyl acetate and recrystallized with MeOH to afford pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08933248B2 |
|---|
| Source dataset | uspto-grants-2015_01 |
|---|
| ORD ID | ord-5dd39c0333bc45c9b481db8caf50b5d0 |
|---|
| Source note | uspto-grants-2015_01 |
|---|
