Nitromethane → HCID 72710224, compound

HRID 1427690Notes

Reaction equation

HRID 1427690 reaction equation
[CH2:1]([N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:11](=[O:12])[C:9]1=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:19]([CH3:22])([O-:21])=[O:20]>O>[CH2:1]([N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:11]([OH:12])([CH2:22][N+:19]([O-:21])=[O:20])[C:9]1=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 6375NitromethaneHCID 2647341-Benzylisatin

Product 1

HCID 72710224HCID 72710224, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
30 °C

Procedure

N-benzyl isatin (0.118 g) and nitromethane (0.15 ml) were added to water and the reaction mixture was vigorously stirred at a temperature of 30° C. for 11 hours. The obtained product was extracted with ethyl acetate and the solvent was removed to give pure product.

Workup

  1. extractionThe obtained product was extracted with ethyl acetate
  2. customthe solvent was removed
  3. customto give pure product

Sources & evidence

ORD record
ord-a78acafda65544a6845df85462c994b4
Source dataset
uspto-grants-2015_01
Patent number
US08933248B2

Reaction notes

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