Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | 1-(2-chlorobenzyl)-1H-indole-2,3-dione | HCID 1581062 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 72709670 | HCID 72709670 | — |
Reaction Steps
1-(2-chlorobenzyl)indoline-2,3-dione (0.135 g) and nitromethane (0.15 ml) were added to water and the reaction mixture was vigorously stirred at a temperature of 30° C. for 9 hours. The obtained product was extracted with ethyl acetate and the solvent was removed to give pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08933248B2 |
|---|
| Source dataset | uspto-grants-2015_01 |
|---|
| ORD ID | ord-5d371e4186424d6da5c917de993e8f83 |
|---|
| Source note | uspto-grants-2015_01 |
|---|
