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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1427695Generated: November 4, 2026

Nitromethane → HCID 72709671, compound

https://huagongshe.com/reaction/1427695

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitromethaneHCID 6375—
ReactantHCID 29299283HCID 29299283—
SolventWaterHCID 962—
ProductHCID 72709671HCID 72709671—

Reaction Conditions

Temperature30 °C

Reaction Steps

1-(4-bromobenzyl)-5-chloroindoline-2,3-dione (0.175 g) and nitromethane (0.15 ml) were added to water and the reaction mixture was vigorously stirred at a temperature of 30° C. for 24 hours. The obtained product was extracted with ethyl acetate and purified by silica gel column chromatography using ethyl acetate/hexane as eluents to afford pure product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08933248B2
Source datasetuspto-grants-2015_01
ORD IDord-f40c312eb78e454da8a0f532f7a9a409
Source noteuspto-grants-2015_01