Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | HCID 2196453 | HCID 2196453 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 72709672 | HCID 72709672 | — |
Reaction Steps
1-(2-chlorobenzyl)-5-chloroindoline-2,3-dione (0.153 g) and nitromethane (0.15 ml) were added to water and the reaction mixture was vigorously stirred at a temperature of 30° C. for 18 hours. The formed solid product was filtered and recrystallized with MeOH to afford pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08933248B2 |
|---|
| Source dataset | uspto-grants-2015_01 |
|---|
| ORD ID | ord-cffa9cbb4f11452a81c75b8f9f2fb6d6 |
|---|
| Source note | uspto-grants-2015_01 |
|---|
