HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46941732, compound → HCID 86682824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46941732 | HCID 46941732 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86682824 | HCID 86682824 | 75.7% |
Reaction Steps
A mixture of [4-(4-fluorophenyl)pyrimidin-5-yl]methanol (4.8 g), manganese dioxide (28 g) and tetrahydrofuran (300 mL) was stirred overnight at room temperature. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (3.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937055B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-3737b5e11db0448bbc0f0aae3b258209 |
| Source note | uspto-grants-2015_01 |