HRID1428222

反应详情

EQUATION

反应方程式

HRID 1428222 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

A solution of 3-chloro-5-(4-methoxy-2-trifluoromethyl-phenylamino)-pyridine-2-carbonitrile (0.64 mmol) in 10 mL ethanol and 0.1 mL hydrochloric acid (37%) was combined with 30 mg of Pd/charcoal (10%) and hydrogenated with stirring at ambient temperature. Then the catalyst was filtered off and the solution was evaporated down. The product thus obtained was reacted further without purification.

WORKUP

后处理

  1. filtrationThen the catalyst was filtered off
  2. customthe solution was evaporated down
  3. customThe product thus obtained
  4. customwas reacted further without purification