Anthracene → HCID 46913382, compound

HRID 1428429Notes

Reaction equation

[CH:1]1[C:14]2[C:5](=[CH:6][C:7]3[C:12]([CH:13]=2)=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:4]=[CH:3][CH:2]=1.[C:15](Cl)(=[O:18])[CH:16]=[CH2:17].[Cl-].[Al+3].[Cl-].[Cl-]>>[C:15]([C:2]1[CH:3]=[CH:4][C:5]2[C:14](=[CH:13][C:12]3[C:7]([CH:6]=2)=[CH:8][CH:9]=[CH:10][CH:11]=3)[CH:1]=1)(=[O:18])[CH:16]=[CH2:17]

Participants

Reactant 3

HCID 8418Anthracene

HCID 13140Acryloyl chloride

HCID 6451240Aluminum(III) Chloride

Product 1

HCID 46913382HCID 46913382, compoundYield 27.5%

Procedure

Anthracene (0.156 g), acryloyl chloride (0.11 g), and aluminium chloride (0.15 g) were treated in the same manner as described in Example 1 to obtain the title compound (56 mg).

Sources & evidence

ORD record: ord-e596e9c8acc1437f9d3b62f581875976
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08937091B2

Reaction notes

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