HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-Chloro-1-(naphthalen-2-yl)propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Naphthalene | HCID 931 | — |
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | 3-Chloro-1-(naphthalen-2-yl)propan-1-one | HCID 12698938 | 38.3% |
Reaction Steps
2-chloroethylpropionyl chloride (2.78 g), naphthalene (2.56 g), and aluminium chloride (3.2 g) were reacted in nitrobenzene (9 mL) at 0° C., followed by treatment with hydrochloric acid to obtain the title compound (1.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-6f584296aa404fb38203d9e4b19fff00 |
| Source note | uspto-grants-2015_01 |