HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-Chloro-1-(4-methylphenyl)propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Nitrobenzene | HCID 7416 | — |
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 3-Chloro-1-(4-methylphenyl)propan-1-one | HCID 235084 | — |
Reaction Steps
2-chloroethylpropionyl chloride (0.63 g), toluene (0.885 g), and aluminium chloride (0.8 g) were reacted in nitrobenzene (1 mL) at 0° C., followed by treatment with hydrochloric acid to obtain the title compound (0.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-4e77235c4727400e95c922968ed11538 |
| Source note | uspto-grants-2015_01 |