HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 2-Methyl-1-phenyl-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | 2-Methyl-1-phenyl-2-propen-1-one | HCID 263666 | — |
Reaction Steps
Benzene (1 mL), methacryloyl chloride (0.156 mg), and aluminium chloride (199 mg) were reacted in carbon disulfide (2 mL) at from 0° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (106 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-1db898b1c6e94443a386b9da369b089f |
| Source note | uspto-grants-2015_01 |