HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Xylene → 1-(2,5-Dimethylphenyl)-2-methyl-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Xylene | HCID 7809 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-(2,5-Dimethylphenyl)-2-methyl-2-propen-1-one | HCID 594429 | — |
Reaction Steps
Paraxylene (1 mL), methacryloyl chloride (110 mg), and aluminium chloride (160 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (140 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-202e3ba202ea4b33a995eccc9c430198 |
| Source note | uspto-grants-2015_01 |