HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Xylene → HCID 24976022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Xylene | HCID 7809 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 24976022 | HCID 24976022 | — |
Reaction Steps
Paraxylene (0.5 mL), methacryloyl chloride (110 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (89 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-9d82a30027b742cd869a3b59be19e35d |
| Source note | uspto-grants-2015_01 |