P-Xylene → HCID 24976022, compound

HRID 1428440Notes

Reaction equation

HRID 1428440 reaction equation
[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([CH3:7])=[CH:3][CH:2]=1.[C:9](Cl)(=[O:13])[C:10](C)=[CH2:11].[Cl-].[Al+3].[Cl-].[Cl-]>ClCCl>[CH3:8][C:1]1[CH:6]=[CH:5][C:4]([CH3:7])=[CH:3][C:2]=1[C:9](=[O:13])[CH:10]=[CH2:11]

Participants

5

Reactant 3

HCID 7809P-XyleneHCID 13528Methacryloyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 24976022HCID 24976022, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Paraxylene (0.5 mL), methacryloyl chloride (110 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (89 mg).

Workup

  1. additionThe resultant was treated in the same manner

Sources & evidence

ORD record
ord-9d82a30027b742cd869a3b59be19e35d
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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